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        關于門尼粘度儀門尼值與門尼應力

        文章作者:admin 上傳更新:2019/1/24 10:43:15 點擊次數:

              使用門尼粘度儀測試的門尼粘度ML(1+4)100℃值是控制天然橡膠加工質量的一個標準,是相對分子質量大小的定性概念。門尼粘度與天然橡膠相對分子質量的定性關系是眾所周知的,如果能夠確定它們之間的定量關系,就可以用常用的門尼粘度儀直接從橡膠干膠的門尼粘度來計算出天然橡膠的相對分子質量,這對于天然橡膠生產農場和橡膠制品廠來說,相對分子質量的測試就是一件很方便很容易的工作了。相對分子質量是天然橡膠的生產部門和研究、使用部門都非常關心的重要參數。已經有很多有效的方法和精密儀器來測試高分子材料的相對分子質量,這些方法在測試相對分子質量前都要用溶劑把待測材料溶解并過濾掉非溶解物和雜質。Mark-Houwink方程η=kMa很好地描述了高分子溶液的粘度與相對分子質量的關系,并在相對分子質量測試中廣泛應用,如果門尼粘度儀該方程也同樣可以描述固體高分子材料的粘度與相對分子質量的關系,就可以直接用固體高分子材料的粘度來表征相對分子質量,從而建立一種方便的相對分子質量測試方法。大多數天然橡膠生產農場和橡膠制品廠都不具備有精密的儀器來測試天然橡膠相對分子質量的條件。

          在相同配方的情況下,門尼粘度儀門尼值高時,物性較好,門尼值低時,物性較差; 門尼值高,對拉力及撕裂有補強效果。門尼值低則相反,如在鞋底配方中,低門尼的配方往往容易“跑”色; 各配合劑分散良好時,門尼值會下降。分散不好,則耐磨性較差;門尼值低,伸長率高時,耐磨性好一些,門尼值用來控制加工性。加工性良好,可保證膠料流注模子內每個角落,而且各種有色膠料的加硫較易掌控,可減少廢料;
          門尼粘度儀門尼應力松弛曲線:
          門尼粘度儀門尼應力松弛之功用:
          傳統之門尼粘度儀只提供門尼粘度值供加工之參考,但以現階段之加工要求這是不夠的,因為門尼粘度只是加熱之后橡膠的流動性,但是外力消失后之回復速度并無法得知,唯有透過應力松弛曲線才得以更精確的控制加工物之尺寸。經由實驗證明有很多的合成物門尼粘度值一樣,但是加工之后尺寸仍不易控制,究其原因就是因為應力松弛之不同造成。
          聚合物材料粘度的測定對選定加工制造方法是很重要的。實際上的測量是在一定的剪切速度W下進行的,例如門尼粘度計和德佛塑性儀。這些方法得到公認,是由于門尼粘度儀具有良好的重現性和在質量控制中的適用價值,但是這些方法不能給出高剪切速度下材料流動特性的任何數據。采用門尼粘度計測定粘度的剪切速度約為25一’仁‘」。但在不同的加工制造過程中,剪切速度高達1055一‘ (表1)。的轉數,試樣會在轉子表面滑動,這時的測量及其結果是不正確的。門尼粘度計中不可能實現高的剪切速度〔2,“·。對于高剪切速度,有效的辦法是采用毛細管流變儀,如孟山都自動毛細管流變儀ARC(圖1)。表1典型的加工過程中的剪切速度1一探測器不攀力P),“一聚合物材料;“一毛細管,4一料筒百加工類型剪切速度,S一’門尼粘度儀模壓塑煉壓出注模1一10210一10名IJ2一了0310呂一10‘如果門尼粘度計中剪切速度超過了轉子 圖1毛細管流變儀 ACR可用于生產控制,也可用于試驗三‘’


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