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        門尼粘度儀與硫化儀的理性分析

        文章作者:admin 上傳更新:2018/12/3 13:16:44 點擊次數:

           門尼粘度儀的重要性主要體現在門尼粘度是衡量橡膠平均分子量及可塑性的一個重要指標,可以反應橡膠加工性能。門尼粘度值高,說明橡膠分子量大,膠料不易混煉均勻及擠出加工;反之,說明橡膠分子量小,膠料易粘輥。門尼粘度過低則硫化后制品抗拉強度低。門尼粘度-時間曲線還能看出膠料硫化工藝性能。



          在我國通常以ML1001+4或者MS1001+4來表示。其中M表示門尼,L表示用大轉子,S表示用小轉子。1表示預熱1分鐘,4表示試驗4分鐘。另外,丁基橡膠、鹵化丁基橡膠和三元乙丙橡膠的實驗溫度采用125℃,丁基橡膠類的讀數時間采用8min.門尼粘度值越大,表示粘度越大,其可塑性越低。



          門尼粘度儀和無轉子硫化儀的區別大致可以分為以下五點:



          無轉子硫化儀與門尼粘度儀外表造型相差無幾,看似一 樣,內部區別是:兩種不同的測試內容。
         

          硫化儀是測定膠料的整個硫化特性的,測試溫度和膠料硫化溫度一樣。硫化儀得到的是一條完整的硫化曲線,在這條曲線上,可以看到正硫化點,也就是得到膠料的正硫化時間。zui大力矩和硬度、定伸強度有關,下模腔來回擺動,帶動膠料正弦振蕩,測定力矩。

          
          門尼粘度儀是測定膠料加工性能的,門尼粘度小,加工時膠料流動性好;門尼儀還可以測定膠料的焦燒時間,焦燒時間是測試膠料安全加工的時間。試驗溫度是100°C,焦燒試驗溫度是120°C。是轉子連續轉動,使膠料連續剪切,測定力矩。


          橡膠硫化儀用于分析、測定橡膠硫化過程的焦燒時間、正硫化時間、硫化速率、粘彈性模量以及硫化平坦期等性能指標,是國家規定用于研制新產品、研究膠料配方及檢驗產品質量的檢測儀器。生產橡膠制品的廠家可以用硫化儀進行制品重現性、穩定性的測試,并進行橡膠配方的設計和檢測。生產廠家可以在生產線上進行現場檢測,掌握每一批、甚至每一時刻橡膠的硫化特性是否滿足制品要求。用來測定未硫化膠料的硫化特性,通過橡膠在模腔內往復振蕩,對模腔的反作用轉矩(力)得到一條轉矩與時間的硫化曲線,科學地確定硫化的時間、溫度、壓力這三大要素,它們是zui終決定產品質量的關鍵,也可測定混煉膠配合的物理性能。原料、加工過程、制成品的質量管理


         
          門尼粘度儀來測定橡膠膠料的可塑性,其測試原理是在一定的溫度、時間和壓力下,測量試樣對轉子轉動所產生的剪切阻力,以扭矩大小的不同來表示膠料可塑度的大小。門尼粘度儀是一個標準的轉子,以恒定的轉速(一般2轉/分),在密閉室的試樣中轉動。轉子轉動所受到的剪切阻力大小與試樣在硫化過程中的粘度變化有關,可通過測力裝置顯示在以門尼為單位的軟件上,以相同時間間隔讀取數值可作出門尼硫化曲線,當門尼數先降后升,從zui低點起上升5個單位時的時間稱門尼焦燒時間,從門尼焦燒點再上升30個單位的時間稱門尼硫化時間。


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